WEF Discussions — Now on LinkedIn!

WEF is pleased to announce the creation of free LinkedIn groups associated with its technical discussion forum topics. Through these LinkedIn groups, members will be able to view and participate in discussions, as well as communicate with one another via direct messages. Share your experiences and knowledge, ask questions and respond to other discussions as frequently as you like!

You must have a LinkedIn profile to join a LinkedIn group; you can create your profile here. If you already have a LinkedIn profile, all you need to do is submit a request to join one or all of the following groups:

Water Environment Federation (Main) | Biosolids | Collection Systems | Nutrients | Stormwater 
Utility Management | Water Reuse | Water for Jobs | Watershed Management | Laboratory Practices 

RSS Feed Print
Ammonia Issues Again
Amy Vail
Posted: Friday, August 12, 2011 10:15 AM
Joined: 8/12/2011
Posts: 1


We do ammonia by ISE.  We were having slope issues so we tried some old probes, same problem.  We bought a new probe, it worked one day and then same issues.  We tried it on another meter, same problems.  Both meters work for ISE for nitrates with no slope issues.  We've used new/old ISA (10N NaOH we make up) and new/old calibration standards.  Any suggestions...I'm running out of scientific method choices.


Dean Falkner
Posted: Sunday, August 28, 2011 8:21 AM
Joined: 6/21/2011
Posts: 11


From past headaches, are you determining the slope following the procedure outlined in the manual or the meter output from running standards?  When we were pushing the lower limit of the probe with our standards, the meter generated slope was beyond the anticipated range.  In talking to tech service, they suggested following the method to determine slope outlined in their manual.  It worked.  They later explained that the slope variability is more when you're using the meter's slope and low level standards.

 

Plan B....check with the manufacturer's technical support.  To facilitate the call, you may want to systematically go through probe troubleshooting procedures and have the answers handy when you make the call.

 

Please let us know the final resolution.  We'll all get stuck there sometime.

 

Dean


James Royer
Posted: Friday, September 16, 2011 3:37 PM
Joined: 9/21/2009
Posts: 98


Are you standards preserved. They will loose strength with time and the the slope is not correct as all the standards are low. It would be impossible to get results then.


nbuske
Posted: Wednesday, October 19, 2011 9:28 AM
Joined: 10/19/2011
Posts: 2


What do all of the probes have in common?  Same lot of ammonia membranes?  Same filling solution?  Do you have another lot that you can try?